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 "inter-"
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Crystal structure and Hirshfeld surface analysis of 3-methyl-4-oxo- N -phenyl-3,4-di-hydro-quinazoline-2-carbo-thio-amide.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Jan 01; Vol. 78 (Pt 1), pp. 47-50. Date of Electronic Publication: 2022 Jan 01 (Print Publication: 2022).

Abstract: The asymmetric unit of the title compound, C 16 H 13 N 3 OS, comprises two mol-ecules ( A and B ) with similar conformations that differ mainly in the orientation of the phenyl group relative to the rest of the mol-ecule, as expressed by the C thio-ami...

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Crystal structure and Hirshfeld surface analysis of 3-[2-(3,5-di-methyl-phen-yl)hydrazinyl-idene]benzo-furan-2(3 H )-one.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2021 Nov 12; Vol. 77 (Pt 12), pp. 1280-1284. Date of Electronic Publication: 2021 Nov 12 (Print Publication: 2021).

Abstract: In the title compound, C 16 H 14 N 2 O 2 , the 2,3-di-hydro-1-benzo-furan ring system is essentially planar and makes a dihedral angle of 3.69 (7)° with the di-methyl-phenyl ring. The mol-ecular conformation is stabilized by an intra-molecular N-H⋯O hy...

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Crystal structure and Hirshfeld surface analysis of ( E )-1-[2,2-di-chloro-1-(4-fluoro-phen-yl)ethen-yl]-2-(2,4-di-chloro-phen-yl)diazene.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2021 Oct 26; Vol. 77 (Pt 11), pp. 1158-1163. Date of Electronic Publication: 2021 Oct 26 (Print Publication: 2021).

Abstract: In the title compound, C 14 H 7 Cl 4 FN 2 , the dihedral angle between the 4-fluoro-phenyl ring and the 2,4-di-chloro-phenyl ring is 46.03 (19)°. In the crystal, the mol-ecules are linked by C-H⋯N inter-actions along the a -axis direction, forming a C ...

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Crystal structure and Hirshfeld surface analysis of ( E )-4-({2,2-di-chloro-1-[4-(di-methyl-amino)-phen-yl]ethenyl}diazen-yl)benzo-nitrile.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2021 Sep 07; Vol. 77 (Pt 10), pp. 994-998. Date of Electronic Publication: 2021 Sep 07 (Print Publication: 2021).

Abstract: In the title compound, C 17 H 14 Cl 2 N 4 , the dihedral angle between the aromatic rings is 50.09 (9)°. The central -N=N- unit shows an E configuration. In the crystal, C-H⋯N inter-actions, C-Cl⋯π and π-π stacking inter-actions [centroid-to-centroid d...

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Crystal structure and Hirshfeld surface analysis of ( E )-1-[2,2-di-chloro-1-(4-methyl-phen-yl)ethen-yl]-2-(4-meth-oxy-phen-yl)diazene.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2021 Aug 27; Vol. 77 (Pt 9), pp. 965-970. Date of Electronic Publication: 2021 Aug 27 (Print Publication: 2021).

Abstract: The asymmetric unit of the title compound, C 16 H 14 Cl 2 N 2 O, comprises two similar mol-ecules, A and B , in which the dihedral angles between the two aromatic rings are 70.1 (3) and 73.2 (2)°, respectively. The crystal structure features short C-H⋯...

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Crystal structure and Hirshfeld surface analysis of bis-(6,7,8,9-tetra-hydro-11 H -pyrido[2,1- b ]quinazolin-5-ium) tetra-chlorido-zincate.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2021 May 14; Vol. 77 (Pt 6), pp. 629-633. Date of Electronic Publication: 2021 May 14 (Print Publication: 2021).

Abstract: The title compound, (C 12 H 15 N 2 ) 2 [ZnCl 4 ], is a salt with two symmetrically independent, essentially planar heterocyclic cations and a slightly distorted tetra-hedral chloro-zincate dianion. N-H⋯Cl hydrogen bonds link these ionic constituents in...

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Crystal structure of 4-(anthracen-9-yl)pyridine.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2021 May 11; Vol. 77 (Pt 6), pp. 605-608. Date of Electronic Publication: 2021 May 11 (Print Publication: 2021).

Abstract: The title compound, C 19 H 13 N, which crystallizes in the monoclinic C 2/ c space group with one half-mol-ecule in the asymmetric unit, was synthesized by Suzuki-Miyaura cross-coupling reaction of 9-bromo-anthracene with pyridin-4-ylboronic acid and p...

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Crystal and mol-ecular structures of di-chlorido-palladium(II) containing 2-methyl- or 2-phenyl-8-(diphenyphosphan-yl)quinoline.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2021 Jan 01; Vol. 77 (Pt 1), pp. 52-57. Date of Electronic Publication: 2021 Jan 01 (Print Publication: 2021).

Abstract: The crystal structures of di-chlorido-palladium(II) complexes bearing 2-methyl- and 2-phenyl-8-(di-phenyl-phosphan-yl)quinoline, namely, di-chlorido-[8-(di-phenyl-phosphan-yl)-2-methyl-quinoline-κ 2 N , P ]palladium(II), [PdCl 2 (C 22 H 18 NP)]...

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Crystal structure and Hirshfeld analysis of di- tert -butyl 2,2'-[(ethyl-aza-nedi-yl)bis-(methyl-ene)]bis-(1 H -pyrrole-1-carboxyl-ate).

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2020 Nov 13; Vol. 76 (Pt 12), pp. 1827-1831. Date of Electronic Publication: 2020 Nov 13 (Print Publication: 2020).

Abstract: The title compound, C 22 H 33 N 3 O 4 , crystallizes in the triclinic space group P with two mol-ecules in a unit cell. The two pyrrole rings are essentially planar (r.m.s. deviation = 0.002 Å) and they form a dihedral angle of 81.24 (10)° with each ot...

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Crystal structure of bis-[μ- N -(η 2 -prop-2-en-1-yl)piperidine-1-carbo-thio-amide-κ 2 S : S ]bis-[(thio-cyanato-κ N )copper(I)].

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2020 Oct 06; Vol. 76 (Pt 11), pp. 1712-1715. Date of Electronic Publication: 2020 Oct 06 (Print Publication: 2020).

Abstract: The title crystalline compound, [Cu 2 (NCS) 2 (C 9 H 16 N 2 ) 2 ], was obtained from the reaction of copper(I) thio-cyanate (CuSCN) with ( N -prop-2-en-1-yl)piperidine-1-carbo-thio-amide as a chelating and bridging thio-urea ligand in chloro-benzene. T...

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