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Crystal structures of ( Z )-(ethene-1,2-di-yl)bis-(di-phenyl-phosphine sulfide) and its complex with Pt II dichloride.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2023 Jan 01; Vol. 79 (Pt 1), pp. 28-32. Date of Electronic Publication: 2023 Jan 01 (Print Publication: 2023).

Abstract: The crystal structures of ( Z )-(ethene-1,2-di-yl)bis-(di-phenyl-phosphine sulfide), C 26 H 22 P 2 S 2 ( I ), along with its complex with Pt II dichloride, di-chlorido[( Z )-(ethene-1,2-di-yl)bis-(di-phenyl-phosphine sulfide)-κ 2 S , S ']platin...

Synthesis, crystal structure and Hirshfeld surface analysis of catena -poly[[bis-(semicarbazide-κ 2 N , O )copper(II)]-μ-sulfato-κ 2 O : O '].

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Oct 20; Vol. 78 (Pt 11), pp. 1131-1134. Date of Electronic Publication: 2022 Oct 20 (Print Publication: 2022).

Abstract: The title polymer, [Cu(SO 4 )(CH 5 N 3 O) 2 ] n , has been synthesized from aqueous solutions of CuSO 4 and semicarbazide. In the crystal structure, the Cu II atoms are chelated by two neutral semicarbazide mol-ecules through the o...

Crystal structure and Hirshfeld surface analysis of 4-(3-meth-oxy-phen-yl)-2,6-di-phenyl-pyridine.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Aug 23; Vol. 78 (Pt 9), pp. 932-935. Date of Electronic Publication: 2022 Aug 23 (Print Publication: 2022).

Abstract: The title compound, C 24 H 19 NO, was obtained via the reaction of (1 E ,2 E )-3-(3-meth-oxy-phen-yl)-1-phenyl-prop-2-en-1-one with ethyl 2-oxo-propano-ate, using NH 4 I as a catalyst. The compound crystallizes in the monoclinic space group I 2/ a . In...

Synthesis and crystal structure of 2-(2-hy-droxy-phen-yl)-1,3-bis-(4-meth-oxy-benz-yl)-1,3-diazinan-5-ol.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Jun 28; Vol. 78 (Pt 7), pp. 742-745. Date of Electronic Publication: 2022 Jun 28 (Print Publication: 2022).

Abstract: The redetermined structure of 2-(2-hy-droxy-phen-yl)-1,3-bis-(4-meth-oxy-benz-yl)-1,3-diazinan-5-ol, C 26 H 30 N 2 O 4 , at 173 K has ortho-rhom-bic ( Pbca ) symmetry. It was previously described by Bolte et al. [ Private Communication (refcode EWICEV)...

Crystal structure and Hirshfeld surface analysis of ( E )-2-(4-bromo-phen-yl)-1-[2,2-di-bromo-1-(4-nitro-phen-yl)ethen-yl]diazene.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Jun 16; Vol. 78 (Pt 7), pp. 732-736. Date of Electronic Publication: 2022 Jun 16 (Print Publication: 2022).

Abstract: The mol-ecule of the title compound, C 14 H 8 Br 3 N 3 O 2 , consists of three almost planar groups: the central di-bromo-ethenyldiazene fragment and two attached aromatic rings. The mean planes of these rings form dihedral angles with the plane of the...

Crystal structure and Hirshfeld surface analysis of 2,2'-(phenyl-aza-nedi-yl)bis-(1-phenyl-ethan-1-one).

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Jun 07; Vol. 78 (Pt 7), pp. 691-694. Date of Electronic Publication: 2022 Jun 07 (Print Publication: 2022).

Abstract: The whole mol-ecule of the title compound, C 22 H 19 NO 2 , is generated by twofold rotational symmetry. The N atom exhibits a trigonal-planar geometry and is located on the twofold rotation axis. In the crystal, mol-ecules are linked by C-H⋯O contacts...

Crystal structure and Hirshfeld surface analysis of ( E )-1-[2,2-di-bromo-1-(4-nitro-phen-yl)ethen-yl]-2-(4-fluoro-phen-yl)diazene.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Apr 28; Vol. 78 (Pt 5), pp. 530-535. Date of Electronic Publication: 2022 Apr 28 (Print Publication: 2022).

Abstract: In the title compound, C 14 H 8 Br 2 FN 3 O 2 , the 4-fluoro-phenyl ring and the nitro-substituted phenyl ring form a dihedral angle of 64.37 (10)°. Mol-ecules in the crystal are connected by C-H⋯O and C-H⋯F hydrogen bonds into layers parallel to (011)...

Crystal structure and Hirshfeld surface analysis of 5-(5-phenyl-1,2-oxazol-3-yl)-1,3,4-thia-diazol-2-amine.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Mar 31; Vol. 78 (Pt 4), pp. 453-457. Date of Electronic Publication: 2022 Mar 31 (Print Publication: 2022).

Abstract: The title compound, C 11 H 8 N 4 OS, crystallizes with two independent mol-ecules in the asymmetric unit. In the crystal, the N-H⋯N and C-H⋯N hydrogen bonds connect the mol-ecules, generating double layers parallel to the (001) plane. The layers are jo...

Crystal structure and Hirshfeld surface analysis of 2-(2-hy-droxy-phen-yl)quinoline-6-sulfonamide.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Mar 17; Vol. 78 (Pt 4), pp. 409-413. Date of Electronic Publication: 2022 Mar 17 (Print Publication: 2022).

Abstract: In the title compound, C 15 H 12 N 2 O 3 S, there are two mol-ecules ( A and B ) in the asymmetric unit. The attached phenol and quinoline moieties of each mol-ecule are almost coplanar with a dihedral angle of 6.05 (15)° for mol-ecule A and 1.89 (13)°...

Crystal structure and Hirshfeld surface analysis of ( E )-1-[2,2-di-bromo-1-(2-nitro-phen-yl)ethen-yl]-2-(4-fluoro-phen-yl)diazene.

Publication Type: Academic Journal

Source(s): Acta crystallographica. Section E, Crystallographic communications [Acta Crystallogr E Crystallogr Commun] 2022 Mar 17; Vol. 78 (Pt 4), pp. 404-408. Date of Electronic Publication: 2022 Mar 17 (Print Publication: 2022).

Abstract: In the title compound, C 14 H 8 Br 2 FN 3 O 2 , the nitro-substituted benzene ring and the 4-fluoro-phenyl ring form a dihedral angle of 65.73 (7)°. In the crystal, mol-ecules are linked into chains by C-H⋯O hydrogen bonds running parallel to the c -ax...

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